RT Journal Article T1 Microwave-assisted reaction sintering of bismuth titanate-based ceramics A1 Azurmendi, Naiara A1 Caro, Iñaki A1 Caballero, Amador C. A1 Jardiel, Teresa A1 Villegas, Marina AB Bismuth titanate-based ceramics, pure and doped with 5 mol% WO3, were prepared by reaction-sintering using a microwave oven. High densities, ≥96% of theoretical density were achieved with very short thermal treatments, with soaking time ranging from 5 to 15 min. Relatively small platelet-like grains were formed, and microstructure seemed not to be strongly affected by doping nor soaking time. Electrical measurements were performed and, as expected, a decrease of electrical conductivity was observed in WO 3-doped materials. The results of reaction-sintered samples, both conventional as well as microwave sintered, are compared with those of samples prepared with previously calcined powders and sintered using microwaves as well as a conventional electric furnace. SN 0002-7820 YR 2006 FD 2006-04 LK https://hdl.handle.net/11556/3781 UL https://hdl.handle.net/11556/3781 LA eng NO Azurmendi , N , Caro , I , Caballero , A C , Jardiel , T & Villegas , M 2006 , ' Microwave-assisted reaction sintering of bismuth titanate-based ceramics ' , Journal of the American Ceramic Society , vol. 89 , no. 4 , pp. 1232-1236 . https://doi.org/10.1111/j.1551-2916.2005.00882.x DS TECNALIA Publications RD 31 jul 2024