%0 Journal Article %A Ocejo, Marta %A Goiti, Eunate %A Salinas-Garzón, Juan %A Ibáñez-Gómez, José Antonio %T Preparation and properties of aluminosilicate aerogels from boehmite and waterglass %D 2024 %@ 0254-0584 %U https://hdl.handle.net/11556/3412 %X Aluminosilicate aerogels are promising thermal insulation materials for high temperature applications. In this study, aluminosilicate aerogels were effectively synthesised using affordable precursors: dispersible boehmite powder and waterglass solutions, with subsequent drying achieved by supercritical CO2 processing. According to the evaluation of their properties, the Al–Si aerogels exhibited low densities (0.11 g/cm3), low thermal conductivities (<0.021 W/m·K) and high specific surface areas (SSA) (516 m2/g for an Al:Si molar ratio of 3:1). When waterglass-based aerogel and aluminosilicate samples were treated at high temperature (1200 °C), the formation of mullite was demonstrated for the aluminosilicate aerogel with a molar ratio of Al:Si 3:1, which showed a higher value for SSA compared to the waterglass-based aerogel. %~