Browsing by Keyword "Tribology"
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Item Nitriding of titanium by hollow cathode assisted active screen plasma and its electro-tribological properties(2021-04-15) Domínguez-Meister, Santiago; Ibáñez, Iñigo; Dianova, Anastasia; Brizuela, Marta; Braceras, Iñigo; Tecnalia Research & Innovation; INGENIERÍA DE SUPERFICIESTitanium presents good corrosion resistance, a high strength-to-weight ratio, but poor tribological properties. However, these can be enhanced by nitriding processes. Hollow cathode assisted active screen plasma has proved to be an effective and fast nitriding technique. In this work, the effect of process parameters (hollow cathode induced temperature and plasma intensity, electrical bias…) on the resulting surface microstructure (XRD, SEM/EDS), finishing and hardness of titanium (TiGr4) have been studied. Additionally, the electro-tribological properties have been evaluated on a ball on cylinder reciprocating configuration. The results show that hollow cathode assisted active screen plasma nitriding of titanium can produce titanium nitride surfaces with thicknesses far exceeding those typical in PVD coatings. Moreover, higher plasma processing intensities can generate same layer thicknesses at lower temperatures, minimizing the deleterious effect on grain size growth. Finally, monitoring of the electrical contact resistance can provide valuable information concerning the evolution of the status of the surfaces.Item Oversizing Thread Diagnosis in Tapping Operation(2021-03-25) Gil Del Val, Alain; Veiga, Fernando; Penalva, Mariluz; Arizmendi, Miguel; Tecnalia Research & Innovation; FABRIC_INTELAutomotive, railway and aerospace sectors require a high level of quality on the thread profiles in their manufacturing systems knowing that the tapping process is a complex manufacturing process and the last operation in a manufacturing cell. Therefore, a multivariate statistical process control chart, for each tap, is presented based on the principal components of the torque signal directly measured from spindle motor drive to diagnosis the thread profile quality. This on-line multivariate control chart has implemented an alarm to avoid defected screw threads (oversized). Therefore, it could work automatically without any operator intervention assessing the thread quality and the safety is guaranteed during the tapping process.Item Tailored synthesis of TiC/a-C nanocomposite tribological coatings(2005-10-25) Martínez-Martínez, D.; López-Cartes, C.; Justo, A.; Fernández, A.; Sánchez-López, J.C.; García-Luis, A.; Brizuela, Marta; Onate, J.I.; TECNOLOGÍAS DE HIDRÓGENO; INGENIERÍA DE SUPERFICIES; Tecnalia Research & InnovationComposite coatings made of nanocrystalline TiC (nc-TiC) particles and amorphous carbon (a-C) have been prepared in a double magnetron sputtering system using graphite and titanium targets under Ar bombardment. Chemical composition and microstructure of coatings were studied by transmission electron microscopy (TEM), electron energy loss spectroscopy (EELS), and x-ray diffraction (XRD) for a set of samples prepared varying the ratio and intensity of power applied to each magnetron. Changes in coatings microstructure, from a quasipolycrystalline TiC to a nanocomposite formed by nanocrystals of TiC embedded in an amorphous matrix of carbon (nc-TiC/a-C), are observed depending on the synthesis conditions. Tribological and mechanical properties of coatings were tested using a pin-on-disk tribometer and an ultramicrohardness indenter, respectively. Coatings with moderate hardness (7-27 GPa), low friction (0.1-0.2), and low wear rates (k similar to 10(-7) mm(3)/N m) were obtained. A percentage between 15% and 30% of TiC is found as an optimum value to get a good compromise between good mechanical and tribological properties. Finally, a mapping of the mechanical and tribological properties of the nc-TiC/a-C system is presented for the synthesis conditions employedItem Tribología de nuevas capas autolubricantes producidas mediante PVD(2005) Oñate, J. I.; Brizuela, M.; Garcĩa-Luis, A.; Braceras, I.; Pacheco, S.; Viviente, J. L.; Tecnalia Research & Innovation; INGENIERÍA DE SUPERFICIES; TECNOLOGÍAS DE HIDRÓGENO; TECNOLOGÍA DE MEMBRANAS E INTENSIFICACIÓN DE PROCESOSLas capas de MoS2 depositadas mediante PVD tienen baja fricción en vacío pero se degradan con facilidad al aire, especialmente en presencia de humedad. Este trabajo describe el desarrollo de nuevas capas de MoS^ modificadas con WC. En ensayos de "bola sobre disco" a 0,75 GPa, las capas presentaron una fricción muy baja y estable (< 0,04) en vacío. Se obtuvo una durabilidad superior a 1 millón de ciclos, mostrando un desgaste de 1,3 X 10e-16 me3 /Nm, mejorado respecto a otras capas de MoS2. El coeficiente de fricción aumentó a 0,15 y la durabilidad disminuyó hasta 1 a 3 x 10e5 ciclos en aire hasta 70 % HR.El análisis superficial mostró ratios de S/Mo superiores a 1,2, con menos del 2 % de oxígeno, demostrando carácter lubricante.Item The vacuum tribology model (VTM) of tribolab(2003) Garmendia, I.; Landaberea, A.; Anglada, E.; Fernández-Sanz, R.; Santiago, R.; Herrada, F.; Encinas, J. M.; CIRMETALTriboLAB is a tribology instrument that is planned for installation in the EuteF Flight Segment Platform [1], along with several other European scientific instruments. Eutef will be fixed onto an Express Pallet Adapter (ExPA), which provides standard structural, mechanical, electrical and communications interfaces to the Columbus External Payload Facility of the International Space Station (ISS). As a part of the model philosophy, a vacuum tribological model (VTM) has been developed to generate "on ground" tribological data of selected lubricants. The idea is to compare the results obtained "on ground" with those that will be produced in the space, in order to investigate the different behaviors of same tribological films and to be able to compare the performance of specific lubricants in Low Earth Orbit (LEO) conditions. The VTM is composed of six double experiment cells that perform respectively ball bearing (BB) experiments (with liquid and solid lubrication) and pin-on-disk (PoD) tests of solid lubricants. Thin films of alloyed MoS 2 are being tested in the VTM under controlled vacuum conditions. In this work, the two sections of the VTM are described.