Tribología de nuevas capas autolubricantes producidas mediante PVD
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2005
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CENIM - CSIC
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Abstract
Las capas de MoS2 depositadas mediante PVD tienen baja fricción en vacío pero se degradan con facilidad al aire, especialmente en presencia de humedad. Este trabajo describe el desarrollo de nuevas capas de MoS^ modificadas con WC. En ensayos de "bola sobre disco" a 0,75 GPa, las capas presentaron una fricción muy baja y estable (< 0,04) en vacío. Se obtuvo una durabilidad superior a 1 millón de ciclos, mostrando un desgaste de 1,3 X 10e-16 me3 /Nm, mejorado respecto a otras capas de MoS2. El coeficiente de fricción aumentó a 0,15 y la durabilidad disminuyó hasta 1 a 3 x 10e5 ciclos en aire hasta 70 % HR.
El análisis superficial mostró ratios de S/Mo superiores a 1,2, con menos del 2 % de oxígeno, demostrando carácter lubricante.
MoS2 coatings, deposited by PVD show a low friction under vacuum conditions, but degrade easily under atmospheric conditions. This work describes the development of a new type of MoSx, coating, modified with WC. These coatings presented a very low and stable friction coefficient lower than 0.04 when tested under vacuum at 0.75 GPa in a ball on disc tribometer. Durability was higher than 1 million wear cycles, showing a wear rate of 1.3 10e-16 m3 /Nm. When tested under atmospheric conditions and up to 70 % RH, friction increased to 0.15 and durability reached a lower value of up to 3 x 10e5 cycles. Surface analyses in these coatings showed S/Mo ratios higher than 1.2 and with oxygen levels lower than 2 %, demonstrating the lubricant character of the coating.
MoS2 coatings, deposited by PVD show a low friction under vacuum conditions, but degrade easily under atmospheric conditions. This work describes the development of a new type of MoSx, coating, modified with WC. These coatings presented a very low and stable friction coefficient lower than 0.04 when tested under vacuum at 0.75 GPa in a ball on disc tribometer. Durability was higher than 1 million wear cycles, showing a wear rate of 1.3 10e-16 m3 /Nm. When tested under atmospheric conditions and up to 70 % RH, friction increased to 0.15 and durability reached a lower value of up to 3 x 10e5 cycles. Surface analyses in these coatings showed S/Mo ratios higher than 1.2 and with oxygen levels lower than 2 %, demonstrating the lubricant character of the coating.
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Revista de Metalurgia - Madrid, Vol 41 no. Extr (2005), pp 148-153